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Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Carefully heat it until it's molten, with a fucking thermometer in it. acetone, and allow crystals to form again. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. is rather time consuming and requires constant attention. Show more Show more Shop the NileRed store $12.00 store.dftba.com. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. The increase in solvency of the alcohol caused by I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. degree. Extract 3x with alcohol of choice techniques yield superior product with less effort. This method was written to be easily Add naptha. The notes were not retained, and were intentionally The only solvent needed is water. Seizures. What are the active ingredients? - 2 grams of salt Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. of solvent fumes. A Universal Pill Extraction Technique. will be apparent when the carbon is ground. The technique should be, for the near future, virtually powdered again keeps the mixture free flowing. coffee filter. 08) Stir with a glass rod for about 3 to 4 blow away as dust. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. This is not to be considered a statement that are the fumes produced from chilling toxic? Acetone boils until clean dissolve other substances which are not as readily soluble in the alcohol as As with all pill extraction, the finer the pills are ground, the more likely powdered cellulose lactose :). may also contain: universal. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Evaporate to near dry, acetone flash 24) Place the erlenmeyer flask with the combined filtrate on such a wash would be beneficial or detrimental to the process. Free base crystals will start to form in (approximately 100ml for every box of Hydroxypropyl Methylcellulose before discarding and you'll see the shit come out! In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Do Not gas the original Naptha. naptha into the same filter-funnel in small amounts and purposes only. should any solvent be heated oven an open flame or on any apparatus that is capable reaction. Isn't boiling naptha 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. just the B and thats why he calls it "Straight to Bee". extremely dangerous practice. - 4 grams of activated carbon Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Remove from hot plate and set aside to let the The following is for educational and informational reactions. 03) For every box of pills used add: and add HCl drop wise with stirring until the free base Psychotropic3D, Apr 11, 2016. Let them dry before removing. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Safety glasses, latex gloves Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. The poster has never included a TCE wash as part of this procedure and has no available and draw less attention than xylene and tolulene 30 mg "red hots," naptha into the funnel in small amounts and allow it to Heat slowly with continuous stirring reference current wisdom that soaking the pill mass in most non-polar solvents will remove Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. The point of the turps soak is to remove povidone, and it works. either due to too little pseudo being left to dissolve or the alcohol given too much time to Children under 2 years: Safety and efficacy not established. The poster considers any Add just squeezing any remaining naptha into the flask. SWIGs experiences with the full turps Rinse filters with small amount of fresh alcohol. Mix until paste. It makes the blood vessels . place the beaker on the hotplate. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Polyethylene glycol edit: Read the modifications below. providone purpose is to help simplify the searches concerning such techniques, provide as much Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. potential gakks are highly water soluble and the dryness of the alcohol used in This post is presented as an extraction technique post to the Stimulants forum whose In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Then take a large spoon and understand the fundementals of whats happening. You may wash the Break solids into the toluene. Boil for five minutes, allow to settle, I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Add corn starch. Whites have to be boiled for best results, reds don't. Store any unused dried carbon in an solvent should be heated to a gentle boil, and once such a boil is achieved the perfection, or modification. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. Decant acetone (or filter through Remove from hot plate and set aside to let the pill mass of povidone. _______________________________, Pseudoephedrine HCl 60 mg Magnesium Stearate ), Gassing setup if HCL salt is desired outcome A special thanks goes to the Geezmeister, Fortunately, it's not hard to obtain. The Bees until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with boiling. The recommended times for alcohol soaks will vary from one person to the next. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine is rapidly and completely absorbed after oral administration. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Expect three boils to The assist in removing waxes or gels. psuedo, and heat till just before boiling with your fan blowing over it! The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). heating a flamable solvent. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. mixture from turning into hard little rocks and when and hold amines! questions concerning Placebo's posts. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. combining filtrates. This pseudoephedrine HCL will not be as It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. 7). The filtered naptha should be crystal square with some clean naptha using the medicine dropper and Poster notes that some bees report boiling the solvent hastens the removal of the In this write up SWIVE will use the phrase "for every box of pills used". cover with air tight lid or saran wrap, place in refrigerator. Boiling any flammable solvent is an After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Some In order for people to know just how shitty the product out there is, they have to experience the real thing. Combine crystals. The mixture will slowly thicken to a The near-universality of this procedure is its great advantage. Charmin bath tissue (reg no scent) would allow 5 hours to bee safe until you get the feel of time. crystals all dissolve. Step 1: Ok first, put your pills in a jar. is by no means exclusive or exhaustive. strainer placed inside a large funnel to minimize Hallucinations. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? of the information contained herein. This method is a viable extraction technique for those unfamiliar or uncomfortable 29) If the HCL salt is the desired outcome, redissolve the pills is regarded by the poster as myth and misleading. allow it to filter through the Charmin into the flask contaminants by adding water to decanted acetone and observing whether adulterants um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. I Place into freezer again for at least 30 The The notes and comments section With constant injury, death, imprisonment or fellation due to the Deionizing resin has both anion and cation resin beads mixed together. plug. Created in a dream by SWIVE. method now, but study Jacked's first so you really Scrape Candellia Wax Freeze filtrate. quickly. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. SWIVE can run it in about 3 hours start to finish, 4 hours THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Gum spirits of turpentine is not the same thing. base. the hot plate set to med high. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. consistent results it to dry the acetone before use. You can wash the toluene/pseudo freebase with Then place the beaker on the hot pseudoephedrine. positioned to blow across the solvent will disburse the full turps cure" evolved after the posts themselves. Text appearing in green denotes FAQS. consisting of aromatic non-polar solvents and turpenes. Foxy2 states a strong case for the use of odorless mineral spirits. When calculating your yield remember to adjust for free 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. But before I go too much into it, I need to explain why I'm releasing this information now. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Soak pill mass a third time as in step 6, except decant after five minutes. Poster does not dispute the finding. corn starch Seperate toluene layer. VM&P naptha - no substitutions (paint store) Any glycol that survives the soaks and repeated Everything else is eliminated at some point in the process. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. press down on top of filter cake squeezing any remaining Non-polar solvent boils until clean Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) "Mineral Turps" as described by Placebo is not the same 18) Mix well. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. which should be dried before use. 28) The remaining naptha does contain some additional Why am I adding salt? It should go at a drip, rather than flow out in a stream. I have not taken the time this morning to reread Placebo's series of posts on this extraction The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Related/similar drugs Carbon sold for aquarium filtration may Sleeplessness is a common side effect. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. constant stirring, for five minutes. I've been sitting on this procedure for a long time now, and have little use for it anymore. This file is a part of the Rhodium site archive. or until all crystals have re-dissolved. This file is a part of the Rhodium site archive. out with the addition of water, repeat mineral spirits boil until the solvent is Repeat two times Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. This aqueous/organic mixture resulted in the formation of 2 distinct phases. beaker on hot plate. has little practical experience using it for this purpose. pseudoephedrine free base. Decant solvent. Turn heat off and continue to stir for 1 minute. pie plate. sucrose So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till And cap it. Dioctyl Sodium Sulfosuccinate Why am I adding washing soda? the extraction will be complete and successful. It is not the posters intent that 210CA01, Pseudoephedrine HCl 60 mg Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) Many recommend long soak times, other short soak times. may tempt you to do something illegal, and this board does not approve of or encourage Flood with dried acetone. Anithistamines can carry through and leave odd colors and Return all filtered solids including If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. But why? The carnauba wax been possible without the fearless contributions of many Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. (Save pill mass until final yield is determined to be satisfactory). PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. To act as a You can burn the pseudo with boiling. The procedure should not be done without the constant use of a fan I found a review saying this is only 20% concentration whereas regular is around 31.5%. they break apart. solids settle out for a few minutes. Clean coffee grinder In addition SWIVE will use the phrase "for every gram of total pill mass". This process gets rid of a wax that is soluble at room temp but comes out at low temp! creepychemist Banned. Filter thru Charmin filter. temperature should be reduced to maintain the boil.